Lesson 9 An anti-vimentin antibody Research Paper

Applied Molecular Cellular Biology

🧠 Main Idea

Researchers discovered that an antibody called LOB7, which binds to the protein vimentin, can boost the formation of capillary-like tubes by human endothelial cells — a key process in angiogenesis (the creation of new blood vessels).


🧩 Background

  • Vimentin = a cytoskeletal protein usually inside cells, maintaining structure and aiding migration.
  • But recent discoveries show extracellular vimentin also plays roles in infection, inflammation, and cell communication.
  • Scientists wanted to learn what extracellular vimentin does — especially in endothelial cells (which line blood vessels).

They used phage display antibody technology to screen for antibodies binding proteins on ageing endothelial cells. 🧫

One antibody, LOB7, stood out for enhancing tube formation — the way endothelial cells mimic tiny blood vessels in lab assays!


🔬 Results

1️⃣ LOB7 was selected

  • 384 antibody clones were screened.
  • LOB7 bound strongly to older endothelial cells (more vimentin on surface).

2️⃣ LOB7 binds vimentin

  • Using immunoprecipitation and mass spectrometry, they confirmed vimentin as the LOB7 target.
  • LOB7 recognized the coil 2 domain of vimentin 🌀, while the standard anti-vimentin antibody (V9) binds its tail.
  • Verified by ELISA and Western blot — clear, specific signal ✅.

3️⃣ Tube formation assay 🧫🌿

  • In a 2D Matrigel assay (a standard test for angiogenesis):
    • HUVEC (human endothelial) cells formed tubes more efficiently when LOB7 was added.
    • After 5 hours → 21% increase in tube formation vs controls.
    • Effect persisted up to 10 hours, gone by 20 hours.
  • No effect on:
    • Migration (scratch assay)
    • Proliferation (BrdU incorporation) → Suggesting the effect is not due to faster growth or movement, but something structural or signaling-based.

💡 Interpretation

  • Binding of LOB7 to vimentin may stabilize focal adhesions (contact points between cells and their matrix), helping cells connect into tubes.
  • This is the first report of an anti-vimentin antibody promoting angiogenesis under normal oxygen conditions (previous studies saw effects only under hypoxia).

⚗️ Methods in a Nutshell

  • Phage display to find LOB7 antibody.
  • Immunoprecipitation + MS to identify vimentin target.
  • Recombinant expression of vimentin fragments to map the binding site.
  • 2D Matrigel angiogenesis assay to test tube formation.
  • Scratch assay and BrdU assay to test migration and proliferation.

🧩 Key Takeaways

FindingMeaning
LOB7 binds extracellular vimentinVimentin has roles outside cells
Tube formation ↑ 21%Vimentin interaction promotes angiogenesis
No change in migration/proliferationEffect likely structural
Binds coil 2 domainNew functional region identified
First such result under normoxiaExpands understanding of extracellular vimentin

🧬 Why It Matters

Vimentin is linked to:

  • Cell motility
  • Wound healing
  • Cancer metastasis
  • Inflammation

Understanding how antibodies like LOB7 modulate vimentin could reveal new therapeutic targets — but also warns that blocking or activating vimentin might have unintended angiogenic effects. ⚠️


👩‍🔬 Authors

Mathias Lindh Jørgensen et al., Aarhus University, Denmark 🇩🇰 Published in Scientific Reports (2017).


🧲 1. Immunoprecipitation

Meaning: A technique that uses an antibody to “pull down” its binding protein from a complex mixture (like a cell lysate). Why used: The authors used the LOB7 antibody to “fish out” its target protein from HUVEC lysates. Purpose in paper: To confirm what protein LOB7 binds to — mass spectrometry showed the pulled-down protein was vimentin.


🧫 2. Anti-vimentin antibody

Meaning: An antibody that recognizes and binds specifically to the protein vimentin. Why used:

  • The new antibody LOB7 is an anti-vimentin antibody they discovered using phage display.
  • The commercial anti-vimentin V9 was used as a control to validate that LOB7 indeed binds vimentin.

🌬️ 3. Does oxygen matter in promoting angiogenesis by anti-vimentin antibody?

Yes. Previous studies showed anti-vimentin peptides only enhanced tube formation under hypoxia (low oxygen). This study found that LOB7 promotes angiogenesis even under normoxic (normal oxygen) conditions. → This shows that vimentin’s angiogenic role doesn’t depend on oxygen stress, broadening its physiological relevance.


🚶‍♀️ 4. Cell motility

Meaning: The ability of cells to move — critical in tissue repair, immune responses, and metastasis. Why mentioned: The authors checked if LOB7 affected cell migration (motility) using a scratch assay. It didn’t. → So the increased tube formation isn’t from faster movement but likely from improved cell–matrix adhesion.


Vimentin is part of the cytoskeleton — it gives cells shape and helps them reorganize.

  • Motility: It interacts with actin and integrins to let cells extend and move.
  • Wound healing: Migrating fibroblasts and endothelial cells upregulate vimentin to repair tissue.
  • Cancer metastasis: Tumor cells expressing vimentin are more mobile and invasive (a marker of epithelial-to-mesenchymal transition).
  • Inflammation: Extracellular vimentin appears on immune cells (macrophages) and helps regulate signaling during immune activation.

🧵 6. Intermediate filament protein

Meaning: One of the three main cytoskeletal systems in cells (along with actin filaments and microtubules). Function: Provides mechanical support and resilience. Vimentin’s role: It’s the major intermediate filament in mesenchymal cells, linking organelles and maintaining cell integrity.


🧬 7. Phage antibody technology

Meaning: A method to discover new antibodies by displaying them on bacteriophage (virus that infects bacteria) surfaces. How it works:

  1. Create a huge library of phages, each expressing a different antibody fragment (scFv).
  2. Expose phages to your target (like endothelial cell membranes).
  3. Wash away non-binders, keep the ones that stick.
  4. Amplify those and repeat for higher specificity. Why used: To find an antibody that binds proteins on ageing endothelial cells — this led to LOB7.

🌤️ 8. Normoxic condition

Meaning: Standard oxygen levels (around 21% O₂), like normal body tissues. Why mentioned: The authors highlight that LOB7 promotes angiogenesis even without hypoxia, unlike prior peptides. → Indicates that extracellular vimentin can drive angiogenesis under physiological oxygen.


⚙️ 9. Citrullination

Meaning: A post-translational modification where the amino acid arginine → citrulline by the enzyme PAD (peptidylarginine deiminase). Effect: Changes protein charge and folding, often affecting immune recognition. Why mentioned: Vimentin can be citrullinated — these modified forms are implicated in rheumatoid arthritis autoantigens.


✂️ 10. “Proteolytic cleavage by specific caspases and calpain further modify vimentin”

Meaning: Enzymes like caspases (active during apoptosis) and calpain (calcium-dependent protease) cut vimentin into fragments. Why important:

  • Changes filament structure.
  • Alters vimentin’s size on Western blots (explains their observed smaller fragments).
  • Indicates regulation of vimentin during cell death or stress.

🔖 11. In vivo biotinylation

Meaning: Tagging cell-surface proteins with biotin while the cells are still intact (“in vivo” here means within living cells in culture). Why: Biotin allows easy purification later using streptavidin beads. Purpose: To selectively label membrane proteins for antibody screening — ensuring LOB7 targets something on the cell surface.


🧪 12. Precipitated proteins

Meaning: Proteins that are pulled out of a solution (e.g., by antibody-bead binding) and separated by centrifugation or magnet. Why mentioned: These were the proteins bound by LOB7 in immunoprecipitation; they were analyzed by SDS-PAGE + silver staining + MS.


⚰️ 13. Caspase activity

Meaning: Caspases are enzymes that execute apoptosis by cutting specific proteins. Connection: Caspases cleave vimentin during apoptosis, changing its size and weakening the cytoskeleton — seen as smaller fragments on Western blot.


🧫 14. ASF-2 cells

Meaning: A human endothelial cell line used in the lab (like HUVEC). Why used: The authors observed that LOB7 binds more strongly to old ASF-2 cells than young ones → suggesting vimentin expression increases with cell age.


🧬 15. Biotin-labelled lysate

Meaning: A lysate (cell extract) containing biotin-tagged surface proteins. Purpose: These biotin-labeled proteins were used to capture antibody-binding targets during the phage selection process.


🧫 16. “Gel was fixed in silver staining”

Meaning: “Fixing” locks proteins into the gel (using ethanol and acid) before staining. Why:

  • Prevents proteins from diffusing out.
  • Improves clarity and sharpness of the silver stain, which is a very sensitive way to visualize proteins (detects nanogram levels). Used here: To visualize the proteins pulled down by LOB7 before cutting out bands for mass spectrometry.

🕸️ 17. Laminin

Meaning: A key extracellular matrix protein forming the basement membrane. Why included: Used as a negative control in ELISA — to ensure LOB7 binds specifically to vimentin, not to other structural proteins like laminin.


🧭 Overall Goal

Find and characterize an antibody that affects tube formation in endothelial cells and identify its target.


🧪 Step-by-Step Flow

StepMethodWhat They DidWhat It Showed
1️⃣ Screening for antibodiesPhage display antibody technologyCreated a large library of phages displaying single-chain antibody fragments (scFv). These were exposed to biotin-labeled membrane proteins from endothelial cells (HUVEC, ASF-2). Non-binders washed away.Found one interesting antibody, LOB7, that bound strongly to aged endothelial cells.
2️⃣ Identify the target of LOB7Immunoprecipitation + Silver stain + Mass spectrometryUsed LOB7 attached to beads to “pull down” its binding partner from cell lysate → separated proteins by SDS-PAGE → silver-stained → sent bands for MS.Identified the pulled-down protein as vimentin.
3️⃣ Confirm the targetWestern blot (with V9 control)Compared bands detected by LOB7 vs known anti-vimentin antibody (V9) in HUVEC lysate and Matrigel.Both detected the same-sized protein → confirmed LOB7 binds vimentin.
4️⃣ Test binding specificityPhage-ELISACoated plates with recombinant vimentin, laminin, and milk (negative controls). Added LOB7 phage.Strong signal only with vimentin → specific binding.
5️⃣ Map where LOB7 binds on vimentinFragment mapping using recombinant vimentin piecesProduced seven vimentin fragments (F1–F7). Tested binding with LOB7 and V9.LOB7 bound coil 2 region (aa 268–396); V9 bound tail region (aa 405–466).
6️⃣ Test biological effect2D Matrigel tube-formation assayGrew HUVEC on Matrigel with or without 0.5 mg/mL LOB7 or control antibody.After 5 h: +21 % tube length with LOB7; effect lasted ≈10 h, gone by 20 h → pro-angiogenic activity.
7️⃣ Rule out indirect effectsScratch (migration) assay + BrdU (proliferation) assayTested if LOB7 made cells move or divide faster.No difference → LOB7 enhances tube organization, not migration or growth.

📊 How to Visualize It

Picture a flow diagram with arrows:

Phage library ↓ (biotin-labeled endothelial proteins) Selection → LOB7 antibody ↓ Immunoprecipitation + Silver stain + MS → Target = Vimentin ↓ ELISA + Western blot → Confirms specificity to vimentin ↓ Fragment mapping → Binding site = Coil 2 domain ↓ Matrigel tube-formation assay → 21 % ↑ tube length (angiogenesis) ↓ Migration & proliferation tests → No effect → direct structural role

Color-code it if you draw it:

  • 🧬 Blue for molecular ID methods (IP, MS, ELISA, WB)
  • 🧫 Green for cell assays (Matrigel, Scratch, BrdU)
  • 🔴 Red for main finding (tube formation ↑ under normoxia)

🔍 Linking Methods to Conclusions

  1. Discovery phase (Phage display → LOB7).
  2. Validation phase (Immunoprecipitation + MS → Vimentin confirmed).
  3. Mapping phase (Fragments → Coil 2 domain).
  4. Functional phase (Tube formation → Angiogenesis effect).
  5. Control phase (Scratch/BrdU → No confounding growth effects).

Together, they proved:

“Binding extracellular vimentin at its coil 2 region by LOB7 promotes endothelial tube formation under normal oxygen conditions.”

Quiz

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